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G.MANI RANJITH
B.PHARM – 7thsemester
DEPARTMENT OF PHARMACEUTICS INCLUDING BIOTECHNOLOGY
DR.KALAM COLLEGE OF PHARMACY
AVANAM – THANJAVUR(D.T)
DEFINITION
History
Need of Shampoo
IDEAL Properties
Cleansing Action
Classification
Raw Materials
Formulation
Manufacturing Process
Quality Control Tests 7-Jul-24 2
G.MANI RANJITH
DEFINITION
A shampoo is a hair care product, typically in the form of
viscous liquid that is used for cleaning hair to remove
dirt, dandruff, pollutants, and other contaminant
particles that gradually builds up in hair.
7-Jul-24 3
G.MANI RANJITH
HISTORY
Shampoo originally meant head massage in several North
Indian languages.
The word is derived form hindi 'champo'.
Before the advent of shampoos, people typically used soap
for personal care.
• Irritating to the eyes
• incompatible with hard water
• dull- looking film on the hair.
However, soap had the distinct disadvantages
In the 1930s the first synthetic detergent shampoo was
introduced, although it had some disadvantages..
7-Jul-24 4
G.MANI RANJITH
Need of shampoo
 The skin on our head produces a
greasy fluid called Sebum.
 It is produced to protect the hair, by
coating itself all over the head.
 This gives the hair a healthy shine
but when secreted in large amount it
makes the hair look dirty.
7-Jul-24 5
G.MANI RANJITH
Ideal
properties
hair smooth and shiny
Foam production
Non irritation to scalp, skin and
eye.
completely, effectively remove
dirt.
pleasant fragrance
Biodegradability
Low toxicity
Slightly acidic (Ph less than 7), -
since a basic environment weakens
the hair by breaking the disulphide
bonds in hair keratin.
7-Jul-24 6
G.MANI RANJITH
Cleansing Action
Clean and smooth hair
The micelles with the oil and dirt eliminating with the water during rinse
The surfactants create micelles around the dirt and oil that are removed from the skin and hair
The surfactants lower the surface tension of the water
Oils and dirts are attached to the skin and hair
7-Jul-24 7
G.MANI RANJITH
CLASSIFICATION
BASED ON
APPEARANCE BASED ON
Use or
function
BASED ON
origin
7-Jul-24 8
G.MANI RANJITH
BASED ON APPEARANCE
Liquid shampoo
or lotion
Powder shampoo Gel shampoo or
solid cream
7-Jul-24 9
G.MANI RANJITH
Based on appearance
Cream shampoo
Oil shampoo
Miscellaneous – Anti
dandruff , medicated
shampoo
7-Jul-24 10
G.MANI RANJITH
Based on use or function
Conditioning
shampoos
Anti dandruff and
therapeutic
shampoos
Baby shampoos
Balancing shampoo
Clarifying shampoo
7-Jul-24 11
G.MANI RANJITH
BASED ON ORIGIN
Herbal
based
Egg
based
7-Jul-24 12
G.MANI RANJITH
The basic ingredients in a shampoo formation are as follows:
1. Water
2. Surfactants: ammonium lauryl sulphate, sodium lauryl sulphate
3. Foam Boosters: betaines or alkanolamides
4. Thickeners: Carboxy methyl cellulose, NaCl
5. Conditioning agents: silicones such as methicone and quarternary agents
6. Preservatives: DMDM Hydantoin and methylparaben.
7. Antidandruff Agents: Selenium sulphide, inc pyrithone, salicylic acid.
7-Jul-24 13
G.MANI RANJITH
Colorants: m-phenylene-diamine.
Opacifiers: Ethylene Glycol Distearate (EDGS)
Fragrance: Limonene, Ethyl isovalerate
Ethyl Isovalerate (apple scent)
Vanillin (Vanilla scent)
Limonene (citrus scent)
7.pH buffers: citric acid
9. Aesthetic Additives:
7-Jul-24 14
G.MANI RANJITH
FORMULATION
7-Jul-24 15
G.MANI RANJITH
7-Jul-24 16
G.MANI RANJITH
7-Jul-24 17
G.MANI RANJITH
7-Jul-24 18
G.MANI RANJITH
7-Jul-24 19
G.MANI RANJITH
Manufacturing process
7-Jul-24 20
G.MANI RANJITH
CREAM SHAMPOO
SLS 38 %
Cetyl alcohol 7 %
water Upto 100 %
Colour ,Perfume q.S
Preservatives q.s
7-Jul-24 21
G.MANI RANJITH
SURFACTANTS
7-Jul-24 22
G.MANI RANJITH
7-Jul-24 23
G.MANI RANJITH
Foam stability test
Dirt dispersion
WETTING ACTION
Viscosity
Ph determination
DETERMINATION OF FREE ALKALI
SKIN IRRITATION TEST
EYE IRRITATION TEST
7-Jul-24 24
G.MANI RANJITH
Foam Stability test
Cylinder
shake
method
50ml of
the 1%
shampoo
solution
put into a
250ml
graduated
cylinder
cover
the
cylinde
r with
hand
shaken
for 10
times
The total
volumes
of the
foam
contents
after 1
minute
shaking
were
recorded
The foam
volume
was
calculated
Foam
should
retain
for at
least
5mins.
7-Jul-24 25
G.MANI RANJITH
DIRT
DISPERSION
The dirt should stay in water portion.
Estimate the amount of Ink in the foam
shake for 5 min
Close the Test tube
one drop of Indian Ink
10ml dirt water
Put two drops of shampoo in a large test tube
7-Jul-24 26
G.MANI RANJITH
WETTING
ACTION
Canvas disk is used, is one inch in diameter
floated on the surface of a solution
Calculate the time required for it to sink is
measured accurately.
7-Jul-24 27
G.MANI RANJITH
VISCOSITY
Clean the Brookfield Viscometer
100ml of shampoo is taken in a
beaker
and spindle is dipped in it for about
5min and then reading is taken.
MARK LOWER MARK
7-Jul-24 28
G.MANI RANJITH
Mix 1 gram of shampoo + 9ml of
water
Determine the pH using PH meter
at 27 degrees Celsius.
7-Jul-24 29
G.MANI RANJITH
DETERMINATION OF FREE ALKALI
10 grams of
sample 100ml
ethanol
Reflux for
15minShake &
frequently at 5
min interval
Add 5ml Barium
chloride to
remove any
traces of
carbonates
Stop Reflux and
allow to cool
few drops of
phenolphthalein
indicator and
titrate with
Sulphuric acid
7-Jul-24 30
G.MANI RANJITH
Draize test.
A set of 6 Rabbits used for testing each material.
Shampoos should be tested only for a short duration
(NMT)4hours as these products come in contact with skin only for a short duration
These preparations are diluted between concentrations of 8 to 10%.
.These patches are then removed
the skin sites are scored for the changes on the surface of the skin like Edema, erythema
formation
. The products are then classified as-mild irritant, moderate and severer
7-Jul-24 31
G.MANI RANJITH
Skin-irritation Test
Eye-Irritancy Test
On the basis of ability to cause injury to Cornea, Iris, Conjunctiva when
the substances is applied to EYE.
The test is carried out on Adult Albino Rabbits.
Ocular reactions are read which unaided Eye.
Readings are made 24,48,72hours at 4 and 7 days after treatment (or)as
long as injury persists
Any preparation is called an Eye Irritant which shows Corneal and Iris
lesions which persists even after 7days.
7-Jul-24 32
G.MANI RANJITH
 DEFINITION
 History
 Need of Shampoo
 IDEAL Properties
 Cleansing Action
 Classification
 Raw Materials
 Formulation
 Manufacturing Process
 Quality Control Tests
7-Jul-24
G.MANI RANJITH 33
Reference:
A handbook of cosmetics – B.M.MITHAL & R.N.SAHA
https://www.slideshare.net/slideshow/shampoo-137227993/137227993
https://www.slideshare.net/slideshow/shampoo-44457202/44457202
https://www.slideshare.net/slideshow/shampoo-202789757/202789757
7-Jul-24
G.MANI RANJITH 34
THANK
YOU
7-Jul-24 35
G.MANI RANJITH

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Shampoo - cosmetics B.pharm mpharam.pptx

  • 1. G.MANI RANJITH B.PHARM – 7thsemester DEPARTMENT OF PHARMACEUTICS INCLUDING BIOTECHNOLOGY DR.KALAM COLLEGE OF PHARMACY AVANAM – THANJAVUR(D.T)
  • 2. DEFINITION History Need of Shampoo IDEAL Properties Cleansing Action Classification Raw Materials Formulation Manufacturing Process Quality Control Tests 7-Jul-24 2 G.MANI RANJITH
  • 3. DEFINITION A shampoo is a hair care product, typically in the form of viscous liquid that is used for cleaning hair to remove dirt, dandruff, pollutants, and other contaminant particles that gradually builds up in hair. 7-Jul-24 3 G.MANI RANJITH
  • 4. HISTORY Shampoo originally meant head massage in several North Indian languages. The word is derived form hindi 'champo'. Before the advent of shampoos, people typically used soap for personal care. • Irritating to the eyes • incompatible with hard water • dull- looking film on the hair. However, soap had the distinct disadvantages In the 1930s the first synthetic detergent shampoo was introduced, although it had some disadvantages.. 7-Jul-24 4 G.MANI RANJITH
  • 5. Need of shampoo  The skin on our head produces a greasy fluid called Sebum.  It is produced to protect the hair, by coating itself all over the head.  This gives the hair a healthy shine but when secreted in large amount it makes the hair look dirty. 7-Jul-24 5 G.MANI RANJITH
  • 6. Ideal properties hair smooth and shiny Foam production Non irritation to scalp, skin and eye. completely, effectively remove dirt. pleasant fragrance Biodegradability Low toxicity Slightly acidic (Ph less than 7), - since a basic environment weakens the hair by breaking the disulphide bonds in hair keratin. 7-Jul-24 6 G.MANI RANJITH
  • 7. Cleansing Action Clean and smooth hair The micelles with the oil and dirt eliminating with the water during rinse The surfactants create micelles around the dirt and oil that are removed from the skin and hair The surfactants lower the surface tension of the water Oils and dirts are attached to the skin and hair 7-Jul-24 7 G.MANI RANJITH
  • 8. CLASSIFICATION BASED ON APPEARANCE BASED ON Use or function BASED ON origin 7-Jul-24 8 G.MANI RANJITH
  • 9. BASED ON APPEARANCE Liquid shampoo or lotion Powder shampoo Gel shampoo or solid cream 7-Jul-24 9 G.MANI RANJITH
  • 10. Based on appearance Cream shampoo Oil shampoo Miscellaneous – Anti dandruff , medicated shampoo 7-Jul-24 10 G.MANI RANJITH
  • 11. Based on use or function Conditioning shampoos Anti dandruff and therapeutic shampoos Baby shampoos Balancing shampoo Clarifying shampoo 7-Jul-24 11 G.MANI RANJITH
  • 13. The basic ingredients in a shampoo formation are as follows: 1. Water 2. Surfactants: ammonium lauryl sulphate, sodium lauryl sulphate 3. Foam Boosters: betaines or alkanolamides 4. Thickeners: Carboxy methyl cellulose, NaCl 5. Conditioning agents: silicones such as methicone and quarternary agents 6. Preservatives: DMDM Hydantoin and methylparaben. 7. Antidandruff Agents: Selenium sulphide, inc pyrithone, salicylic acid. 7-Jul-24 13 G.MANI RANJITH
  • 14. Colorants: m-phenylene-diamine. Opacifiers: Ethylene Glycol Distearate (EDGS) Fragrance: Limonene, Ethyl isovalerate Ethyl Isovalerate (apple scent) Vanillin (Vanilla scent) Limonene (citrus scent) 7.pH buffers: citric acid 9. Aesthetic Additives: 7-Jul-24 14 G.MANI RANJITH
  • 21. CREAM SHAMPOO SLS 38 % Cetyl alcohol 7 % water Upto 100 % Colour ,Perfume q.S Preservatives q.s 7-Jul-24 21 G.MANI RANJITH
  • 24. Foam stability test Dirt dispersion WETTING ACTION Viscosity Ph determination DETERMINATION OF FREE ALKALI SKIN IRRITATION TEST EYE IRRITATION TEST 7-Jul-24 24 G.MANI RANJITH
  • 25. Foam Stability test Cylinder shake method 50ml of the 1% shampoo solution put into a 250ml graduated cylinder cover the cylinde r with hand shaken for 10 times The total volumes of the foam contents after 1 minute shaking were recorded The foam volume was calculated Foam should retain for at least 5mins. 7-Jul-24 25 G.MANI RANJITH
  • 26. DIRT DISPERSION The dirt should stay in water portion. Estimate the amount of Ink in the foam shake for 5 min Close the Test tube one drop of Indian Ink 10ml dirt water Put two drops of shampoo in a large test tube 7-Jul-24 26 G.MANI RANJITH
  • 27. WETTING ACTION Canvas disk is used, is one inch in diameter floated on the surface of a solution Calculate the time required for it to sink is measured accurately. 7-Jul-24 27 G.MANI RANJITH
  • 28. VISCOSITY Clean the Brookfield Viscometer 100ml of shampoo is taken in a beaker and spindle is dipped in it for about 5min and then reading is taken. MARK LOWER MARK 7-Jul-24 28 G.MANI RANJITH
  • 29. Mix 1 gram of shampoo + 9ml of water Determine the pH using PH meter at 27 degrees Celsius. 7-Jul-24 29 G.MANI RANJITH
  • 30. DETERMINATION OF FREE ALKALI 10 grams of sample 100ml ethanol Reflux for 15minShake & frequently at 5 min interval Add 5ml Barium chloride to remove any traces of carbonates Stop Reflux and allow to cool few drops of phenolphthalein indicator and titrate with Sulphuric acid 7-Jul-24 30 G.MANI RANJITH
  • 31. Draize test. A set of 6 Rabbits used for testing each material. Shampoos should be tested only for a short duration (NMT)4hours as these products come in contact with skin only for a short duration These preparations are diluted between concentrations of 8 to 10%. .These patches are then removed the skin sites are scored for the changes on the surface of the skin like Edema, erythema formation . The products are then classified as-mild irritant, moderate and severer 7-Jul-24 31 G.MANI RANJITH Skin-irritation Test
  • 32. Eye-Irritancy Test On the basis of ability to cause injury to Cornea, Iris, Conjunctiva when the substances is applied to EYE. The test is carried out on Adult Albino Rabbits. Ocular reactions are read which unaided Eye. Readings are made 24,48,72hours at 4 and 7 days after treatment (or)as long as injury persists Any preparation is called an Eye Irritant which shows Corneal and Iris lesions which persists even after 7days. 7-Jul-24 32 G.MANI RANJITH
  • 33.  DEFINITION  History  Need of Shampoo  IDEAL Properties  Cleansing Action  Classification  Raw Materials  Formulation  Manufacturing Process  Quality Control Tests 7-Jul-24 G.MANI RANJITH 33
  • 34. Reference: A handbook of cosmetics – B.M.MITHAL & R.N.SAHA https://www.slideshare.net/slideshow/shampoo-137227993/137227993 https://www.slideshare.net/slideshow/shampoo-44457202/44457202 https://www.slideshare.net/slideshow/shampoo-202789757/202789757 7-Jul-24 G.MANI RANJITH 34