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Separations, Volume 11, Issue 7 (July 2024) – 28 articles

Cover Story (view full-size image): Thallium is an accumulative toxic metal that can be present in environmental samples, and its determination in trace levels is necessary. Lab-in-syringe (LIS) is a simple, functional, and versatile technique that combines the operation concepts of flow and sequential injection analysis. In this work, a liquid-phase microextraction LIS system was developed as a front-end to flame atomic absorption spectrometry for the determination of thallium in water samples. Among the benefits of the method are its handling simplicity, the good figures of merit, and the increased operator’s safety. Due to the decreased chemical consumption, the novel system complies with many requirements of green analytical chemistry and green sample preparation, while it ensures high applicability. View this paper
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