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Leaf tissue metabolomics fingerprinting of Citronella gongonha Mart. by 1H HR-MAS NMR
This research characterizes key metabolites in the leaf from Citronella gongonha Martius (Mart.) Howard (Cardiopteridaceae). All metabolites were...
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Functional control of a 0.5 MDa TET aminopeptidase by a flexible loop revealed by MAS NMR
Large oligomeric enzymes control a myriad of cellular processes, from protein synthesis and degradation to metabolism. The 0.5 MDa large TET2...
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Grading of endometrial cancer using 1H HR-MAS NMR-based metabolomics
The tissue metabolomic characteristics associated with endometrial cancer (EC) at different grades were studied using high resolution (400 MHz) magic...
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Shared and unique metabolic features of the malignant and benign thyroid lesions determined with use of 1H HR MAS NMR spectroscopy
The purpose of this work was to investigate the distinct and common metabolic features of the malignant and benign thyroid lesions in reference to...
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Magic-angle-spinning NMR structure of the kinesin-1 motor domain assembled with microtubules reveals the elusive neck linker orientation
Microtubules (MTs) and their associated proteins play essential roles in maintaining cell structure, organelle transport, cell motility, and cell...
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Atomic-level structure determination of amorphous molecular solids by NMR
Structure determination of amorphous materials remains challenging, owing to the disorder inherent to these materials. Nuclear magnetic resonance...
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Structural characterization of tin in toothpaste by dynamic nuclear polarization enhanced 119Sn solid-state NMR spectroscopy
Stannous fluoride (SnF 2 ) is an effective fluoride source and antimicrobial agent that is widely used in commercial toothpaste formulations. The...
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Revealing carbon capture chemistry with 17-oxygen NMR spectroscopy
Carbon dioxide capture is essential to achieve net-zero emissions. A hurdle to the design of improved capture materials is the lack of adequate tools...
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200 GHz single chip microsystems for dynamic nuclear polarization enhanced NMR spectroscopy
Dynamic nuclear polarization (DNP) is one of the most powerful and versatile hyperpolarization methods to enhance nuclear magnetic resonance (NMR)...
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Spectroscopic identification of Ca-bearing uranyl silicates formed in C–S–H systems
Portland cement-based grouts used for radioactive waste immobilisation contain a Ca- and Si-rich binder phase, known as calcium–silicate–hydrate...
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Enlarging the scenario of site directed 19F labeling for NMR spectroscopy of biomolecules
The possibility of using selectively incorporated 19 F nuclei for NMR spectroscopic studies has retrieved increasing interest in recent years. The...
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Multinuclear 1D and 2D NMR with 19F-Photo-CIDNP hyperpolarization in a microfluidic chip with untuned microcoil
Nuclear Magnetic Resonance (NMR) spectroscopy is a most powerful molecular characterization and quantification technique, yet two major persistent...
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Insights into memory effect mechanisms of layered double hydroxides with solid-state NMR spectroscopy
Layered double oxides (LDOs) can restore the parent layered double hydroxides (LDHs) structure under hydrous conditions, and this “memory effect”...
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Magic angle spinning NMR structure of human cofilin-2 assembled on actin filaments reveals isoform-specific conformation and binding mode
Actin polymerization dynamics regulated by actin-binding proteins are essential for various cellular functions. The cofilin family of proteins are...
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Molecular elucidation of drug-induced abnormal assemblies of the hepatitis B virus capsid protein by solid-state NMR
Hepatitis B virus (HBV) capsid assembly modulators (CAMs) represent a recent class of anti-HBV antivirals. CAMs disturb proper nucleocapsid assembly,...
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Hidden chemical order in disordered Ba7Nb4MoO20 revealed by resonant X-ray diffraction and solid-state NMR
The chemical order and disorder of solids have a decisive influence on the material properties. There are numerous materials exhibiting chemical...
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Molecular identification and quantification of defect sites in metal-organic frameworks with NMR probe molecules
The defects in metal-organic frameworks (MOFs) can dramatically alter their pore structure and chemical properties. However, it has been a great...
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Direct investigation of the reorientational dynamics of A-site cations in 2D organic-inorganic hybrid perovskite by solid-state NMR
Limited methods are available for investigating the reorientational dynamics of A-site cations in two-dimensional organic–inorganic hybrid...
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Accessing Methyl Groups in Proteins via 1H-detected MAS Solid-state NMR Spectroscopy Employing Random Protonation
We recently introduced RAP (reduced adjoining protonation) labelling as an easy to implement and cost-effective strategy to yield selectively methyl...
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Spatially-resolved metabolic profiling of living Drosophila in neurodegenerative conditions using 1H magic angle spinning NMR
Drosophila flies are versatile animal models for the study of gene mutations in neuronal pathologies. Their small size allows performing in vivo ...
